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Airtight Ball Mill

The mixture was then transferred to an airtight ball mill pot along with 5 ml of n-heptane solution and 25 irconia balls 10 mm diameter. Ball mill reaction was carried out at 400 rpm for 12 h in Fritsch Pulverisette equipment. To prevent overheating n-heptane was added. In addition after every 30 min of milling 15 min rest was applied to

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